Accredited calibration services: 

Temperature calibration

From -196oC to 1000oC   ASTM thermometers, digital thermometers, PRTs, thermocouples, thermistors

Hydrometer calibration

Specific Gravity hydrometers. API hydrometers, Baume hydrometers,
Kg/M3 (density) hydrometers, Brix hydrometers, Proof hydrometers

Mass (weight) calibration

ASTM Class 1 and OIML E-2 and lesser specification stainless steel and brass laboratory weights.  New calibrated weights and re-calibration of weights you currently have.

Humidity calibration

Thermo-hygrometers, chart recorders, humidity sensors, data-loggers

Volumetric calibration

Burets, pipets, volumetric flasks, graduated cylinders, volumetric glassware

Verification services

 Testing and certification that an instrument complies with specified accuracy requirements...

Recalibration

Our A2LA Scope

About ICL-Company info

Forms & downloads

FAQs and help topics

Sample reports

Request catalog

 

VOLUMETRIC GLASSWARE CALIBRATION

Many quality systems now require that volumetric glassware be calibrated or certified (the terms are often used interchangeably) where precise measurements are of critical importance. Accordingly, ICL maintains a modern, well equipped volumetric laboratory.

Our calibration capabilities cover graduated glass volumetric ware with capacities from 0.1 ml to 1500 ml.

Mohr Pipets, Volumetric Pipets
Burets
Graduated cylinders
Volumetric flasks
Centrifuge tubes

Please see our A2LA Certificate & Scope of Accreditation for measurement uncertainties.

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CALIBRATION of volumetric ware consists of the following services:

1) The instrument is inspected visually for defects in numbering, graduating, or any obvious physical defects.

2) The instrument is examined under a polariscope to be certain it is free from strains in the glass (usually from the manufacturing process), as severe strains may affect the integrity of the instrument in the long term.

 

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3) In a pipette or other artifact with a precision bore, the bore will be examined under magnification for irregularity in shape or any other defect which would render the instrument unsuitable for certification.

4) If the instrument does not have a serial number, a ceramic decal serial number will be affixed.

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5) The instrument is next carefully cleaned, using solvents or detergents as appropriate, and rinsed with alcohol, then with water, and finally with distilled water, and thoroughly dried by positive ventilation using filtered air.

6) The device is then tested per ICL procedure 03, based on ASTM E-542, as appropriate for the volumes to be contained or delivered.

The meniscus is carefully set at each test point and the quantity of distilled water contained (or delivered) is carefully weighed.  Water temperature is measured to the nearest 0.01oC both before and after the measurement and the average is utilized for the calculations.

The weighing results are then corrected for temperature, and an air buoyancy correction,  based upon current air density (a function of temperature, humidity and atmospheric pressure) is calculated and applied..

Each test point is calibrated a minimum of three times.  The standard deviation of the results must be appropriate for the precision of the device, or additional repetitions are required until the desired level of precision is achieved.


7) A calibration report is prepared detailing all pertinent information concerning the test, the actual volumes contained or delivered, (with corresponding corrections), and all the required information to convey NIST traceability. (See photo at right, below)

All certificates are laminated in heavy plastic for protection in the laboratory environment.

8) A durable calibration tag is affixed to the artifact indicating the date of most recent calibration and the ‘next due’ date.

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9) We will notify you by fax when your instrument is due for recalibration. (One less thing for you to remember)

PRICING: Prices indicated are per point tested. Minimum charge per device tested: $110.00

Prices include pre-calibration examination, calibration, and issuance of report document.

$47.50 per test point

$142.50 for a typical 3 point test on an item

Items with a single test point, such as volumetric flasks: $110.00

  

Sample calibration report for volumetric flask

Recalibration form and address label to send in your instrument for calibration

 

    

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